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Imaging the Meissner effect in hydride superconductors using quantum sensors
In order to explore superconductivity in hydride materials, local magnetometry inside a diamond anvil cell is performed with sub-micron spatial resolution at megabar pressures using nitrogen-vacancy colour centres.
- P. Bhattacharyya
- , W. Chen
- & N. Y. Yao
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Article |
Visualizing interfacial collective reaction behaviour of Li–S batteries
In situ liquid-cell electrochemical transmission electron microscopy allows the direct visualization of the transformation of lithium polysulfides over electrode surfaces at the atomic scale, leading to a new energy-storage mechanism in lithium–sulfur batteries.
- Shiyuan Zhou
- , Jie Shi
- & Hong-Gang Liao
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Article |
Ultrafast deposition of faceted lithium polyhedra by outpacing SEI formation
We report the discovery of lithium metal’s intrinsic growth morphology, a rhombic dodecahedron, and leverage these rhombic dodecahedra as nucleation seeds for improved battery performance.
- Xintong Yuan
- , Bo Liu
- & Yuzhang Li
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Article |
Tracking cubic ice at molecular resolution
Tracking the formation of cubic ice (ice Ic) using transmission electron microscopy and low-dose imaging shows preferential nucleation of ice Ic at low-temperature interfaces and two types of stacking disorder.
- Xudan Huang
- , Lifen Wang
- & Xuedong Bai
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Article |
Photonically active bowtie nanoassemblies with chirality continuum
Self-limited assembly of 'imperfect' chiral nanoparticles enables formation of bowtie-shaped microparticles with size monodispersity and continuously variable chirality to be used for printing photonically active metasurfaces.
- Prashant Kumar
- , Thi Vo
- & Nicholas A. Kotov
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Article
| Open AccessCoherent correlation imaging for resolving fluctuating states of matter
Nanoscale magnetic fluctuations are spatiotemporally resolved beyond conventional resolution limits using coherent correlation imaging, in which frames in Fourier space are recorded and analysed using an iterative hierarchical clustering algorithm.
- Christopher Klose
- , Felix Büttner
- & Bastian Pfau
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Article
| Open AccessAn integrated imaging sensor for aberration-corrected 3D photography
A meta-imaging sensor detects an extra-fine 4D light field distribution using a vibrating microlens array, enabling high-resolution 3D photography up to a gigapixel with fast aberration correction, demonstrated on a telescope aimed at the Moon.
- Jiamin Wu
- , Yuduo Guo
- & Qionghai Dai
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Article |
Spatiotemporal imaging of charge transfer in photocatalyst particles
Photovoltage measurements on cuprous oxide photocatalyst particles are used to spatiotemporally track the charge transfer processes on the femtosecond to second timescale at the single-particle level.
- Ruotian Chen
- , Zefeng Ren
- & Can Li
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Article |
Tracking single adatoms in liquid in a transmission electron microscope
The ability to resolve single atoms in a liquid environment is demonstrated by combining a transmission electron microscope and a robust double graphene liquid cell, enabling studies of adatom motion at solid–liquid interfaces.
- Nick Clark
- , Daniel J. Kelly
- & Sarah J. Haigh
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Article |
Atomic imaging of zeolite-confined single molecules by electron microscopy
Using integrated differential phase contrast scanning transmission electron microscopy, the atomic imaging of single pyridine and thiophene molecules identifies host–guest interactions in zeolite ZSM-5 and their adsorption and desorption behaviours can be studied.
- Boyuan Shen
- , Huiqiu Wang
- & Fei Wei
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Article |
Local nanoscale phase impurities are degradation sites in halide perovskites
A multimodal microscopy toolkit reveals nanoscale defect clusters in halide perovskite films and that these clusters are sites at which photochemical degradation seeds.
- Stuart Macpherson
- , Tiarnan A. S. Doherty
- & Samuel D. Stranks
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Article |
Observation of a molecular bond between ions and Rydberg atoms
A study reports on the observation of a new type of molecular bond between an ion and a Rydberg atom and characterizes the resulting molecule using an ion microscope study.
- Nicolas Zuber
- , Viraatt S. V. Anasuri
- & Tilman Pfau
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Article |
Imaging tunable quantum Hall broken-symmetry orders in graphene
Three tunable quantum Hall broken-symmetry states in charge-neutral graphene are identified by visualizing their lattice-scale order with scanning tunnelling microscopy and spectroscopy.
- Alexis Coissard
- , David Wander
- & Benjamin Sacépé
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Article |
Observing polymerization in 2D dynamic covalent polymers
In situ scanning tunnelling microscopy reveals the dynamic nature of the early stages of two-dimensional (2D) polymer formation and crystallization at the solid–liquid interface.
- Gaolei Zhan
- , Zhen-Feng Cai
- & Steven De Feyter
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Article |
Imaging of isotope diffusion using atomic-scale vibrational spectroscopy
Vibrational electron energy-loss spectroscopy is used to distinguish two stable isotopes of carbon and to monitor their diffusion with subnanometre spatial resolution.
- Ryosuke Senga
- , Yung-Chang Lin
- & Kazu Suenaga
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Article |
Localization atomic force microscopy
A localization algorithm is applied to datasets obtained with conventional and high-speed atomic force microscopy to increase image resolution beyond the limits set by the radius of the tip used.
- George R. Heath
- , Ekaterina Kots
- & Simon Scheuring
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Article |
Long-range nontopological edge currents in charge-neutral graphene
Nanoscale imaging of edge currents in charge-neutral graphene shows that charge accumulation can explain various exotic nonlocal transport measurements, bringing into question some theories about their origins.
- A. Aharon-Steinberg
- , A. Marguerite
- & E. Zeldov
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Article |
High-resolution X-ray luminescence extension imaging
Using lanthanide-doped nanomaterials and flexible substrates, an approach that enables flat-panel-free, high-resolution, three-dimensional imaging is demonstrated and termed X-ray luminescence extension imaging.
- Xiangyu Ou
- , Xian Qin
- & Xiaogang Liu
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Article |
The Philae lander reveals low-strength primitive ice inside cometary boulders
When the Philae lander bounced on the surface of comet 67P/Churyumov–Gerasimenko, it exposed primitive icy-dust material within cometary boulders; the intrinsic strength and porosity of this material is reported.
- Laurence O’Rourke
- , Philip Heinisch
- & Holger Sierks
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Article |
Imaging single glycans
An imaging method combining soft-landing electrospray ion beam deposition and low-temperature scanning tunnelling microscopy resolves the structures of glycans at sub-nanometre resolution, revealing the connectivity of glycan chains and the types of linkages.
- X. Wu
- , M. Delbianco
- & K. Kern
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Article |
Real-space charge-density imaging with sub-ångström resolution by four-dimensional electron microscopy
A real-space imaging technique that combines scanning transmission electron microscopy with an angle-resolved pixellated fast-electron detector is used to image the charge distribution in SrTiO3, BiFeO3 and the junction between them.
- Wenpei Gao
- , Christopher Addiego
- & Xiaoqing Pan
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Letter |
Observing crystal nucleation in four dimensions using atomic electron tomography
Atomic electron tomography captures crystal nucleation in four dimensions in FePt nanoparticles, with the observed early-stage nucleation not consistent with classical nucleation theory.
- Jihan Zhou
- , Yongsoo Yang
- & Jianwei Miao
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Letter |
Needle-like structures discovered on positively charged lightning branches
Radio interferometric observations of lightning over the Netherlands reveal small needle-shaped plasma structures associated with the positive leader channels, explaining why cloud-to-ground lightning connects to the ground multiple times.
- B. M. Hare
- , O. Scholten
- & P. Zucca
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Letter |
Extreme-ultraviolet refractive optics
A refractive lens and a refractive prism for extreme-ultraviolet radiation have been developed that use the deflection of the radiation in an inhomogeneous jet of atoms.
- L. Drescher
- , O. Kornilov
- & B. Schütte
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Article |
Electron ptychography of 2D materials to deep sub-ångström resolution
Combining an electron microscope pixel-array detector that collects the entire distribution of scattered electrons with full-field ptychography greatly improves image resolution and contrast compared to traditional techniques, even at low beam energies.
- Yi Jiang
- , Zhen Chen
- & David A. Muller
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Letter |
Self-assembly of highly symmetrical, ultrasmall inorganic cages directed by surfactant micelles
Machine-learning algorithms are used to generate single-particle three-dimensional reconstructions, revealing that highly symmetrical dodecahedral silica cages, around 10 nm in size, self-assemble in the presence of surfactant micelles.
- Kai Ma
- , Yunye Gong
- & Ulrich Wiesner
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Letter |
Moving magnetoencephalography towards real-world applications with a wearable system
A new magnetoencephalography system allows high-spatiotemporal-resolution imaging of human brain function in moving subjects.
- Elena Boto
- , Niall Holmes
- & Matthew J. Brookes
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Letter |
Real-space imaging of non-collinear antiferromagnetic order with a single-spin magnetometer
A non-invasive scanning magnetometer, based on a single nitrogen–vacancy defect in diamond, visualizes antiferromagnetic order at the nanometre scale in thin films of bismuth ferrite at room temperature.
- I. Gross
- , W. Akhtar
- & V. Jacques
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Letter |
Three-dimensional magnetization structures revealed with X-ray vector nanotomography
Techniques exist for imaging the magnetization patterns of magnetic thin films and at the surfaces of magnets, but here hard-X-ray tomography is used to image the three-dimensional magnetic structure within a micrometre-sized magnet in the vicinity of Bloch points.
- Claire Donnelly
- , Manuel Guizar-Sicairos
- & Laura J. Heyderman
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Letter |
Whole-brain serial-section electron microscopy in larval zebrafish
A complete larval zebrafish brain is examined and its myelinated axons reconstructed using serial-section electron microscopy, revealing remarkable symmetry and providing a valuable resource.
- David Grant Colburn Hildebrand
- , Marcelo Cicconet
- & Florian Engert
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Letter |
Mapping vibrational surface and bulk modes in a single nanocube
Spatial mapping of optical and acoustic, bulk and surface vibrational modes in magnesium oxide nanocubes is demonstrated using a single electron probe.
- Maureen J. Lagos
- , Andreas Trügler
- & Philip E. Batson
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Letter |
High-resolution non-destructive three-dimensional imaging of integrated circuits
A recently developed computational imaging technique, X-ray ptychographic tomography, is used to study integrated circuits, and a 3D image of a processor chip with a resolution of 14.6 nm is obtained.
- Mirko Holler
- , Manuel Guizar-Sicairos
- & Gabriel Aeppli
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Letter |
Amplified stimulated emission in upconversion nanoparticles for super-resolution nanoscopy
Super-resolution optical microscopy based on stimulated emission depletion effects can now be performed at much lower light intensities than before by using bright upconversion emission from thulium-doped nanoparticles.
- Yujia Liu
- , Yiqing Lu
- & Dayong Jin
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Letter |
Deciphering chemical order/disorder and material properties at the single-atom level
The three-dimensional coordinates of more than 23,000 atoms in an iron-platinum nanoparticle are determined with 22 picometre precision to correlate chemical order/disorder and crystal defects with magnetic properties.
- Yongsoo Yang
- , Chien-Chun Chen
- & Jianwei Miao
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Letter |
Nanoscale thermal imaging of dissipation in quantum systems
A cryogenic thermal imaging technique that uses a superconducting quantum interference device fabricated on the tip of a sharp pipette can be used to image the thermal signature of extremely low power nanometre-scale dissipation processes.
- D. Halbertal
- , J. Cuppens
- & E. Zeldov
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Letter |
Quantifying crater production and regolith overturn on the Moon with temporal imaging
High-resolution ‘before and after’ imaging of the Moon is used to quantify the rate of crater production and provide insights into the cratering process.
- Emerson J. Speyerer
- , Reinhold Z. Povilaitis
- & Robert V. Wagner
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Letter |
Engineering and mapping nanocavity emission via precision placement of DNA origami
The incorporation of large numbers of chemically diverse functional components into microfabricated structures at precise locations is challenging; now the precision placement of DNA origami by directed self-assembly is shown to overcome this problem for the purpose of reliably and controllably coupling molecular emitters to photonic crystal cavities.
- Ashwin Gopinath
- , Evan Miyazono
- & Paul W. K. Rothemund
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Letter |
Ultrafast ultrasound localization microscopy for deep super-resolution vascular imaging
Conventional clinical ultrasound imaging has, at best, sub-millimetre-scale resolution, but now a new ultrasound technique is demonstrated that is based on fast tracking of transient signals from a sub-wavelength contrast agent and has sufficiently high resolution to map the microvasculature deep into organs.
- Claudia Errico
- , Juliette Pierre
- & Mickael Tanter
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Letter |
Nanostructure surveys of macroscopic specimens by small-angle scattering tensor tomography
An imaging method that combines small-angle X-ray scattering with tensor tomography to probe nanoscale structures in macroscopic samples is introduced and demonstrated by measuring the main orientation and the degree of orientation of nanoscale mineralized collagen fibrils in a human trabecula bone sample.
- Marianne Liebi
- , Marios Georgiadis
- & Manuel Guizar-Sicairos
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Article |
A zero-knowledge protocol for nuclear warhead verification
Future rounds of nuclear arms control would ideally involve direct inspection of nuclear warheads using procedures that give inspectors high confidence about the authenticity of submitted nuclear items yet give no information about their design; this is now shown to be achievable using zero-knowledge protocols in neutron imaging of nuclear warheads.
- Alexander Glaser
- , Boaz Barak
- & Robert J. Goldston
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Letter |
Three-dimensional imaging of localized surface plasmon resonances of metal nanoparticles
Localized surface plasmon resonances of an individual silver nanocube are reconstructed in three dimensions using electron energy-loss spectrum imaging, resulting in a better understanding of the optical response of noble-metal nanoparticles.
- Olivia Nicoletti
- , Francisco de la Peña
- & Paul A. Midgley
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Letter |
Optical magnetic imaging of living cells
A diamond chip with nitrogen–vacancy centres is used for magnetic imaging of living magnetotactic bacteria with sub-cellular spatial resolution.
- D. Le Sage
- , K. Arai
- & R. L. Walsworth
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Letter |
Mapping molecular motions leading to charge delocalization with ultrabright electrons
An ultrabright femtosecond electron source is used to monitor the molecular motions in the organic salt (EDO-TTF)2PF6 as it undergoes its photo-induced insulator-to-metal phase transition.
- Meng Gao
- , Cheng Lu
- & R. J. Dwayne Miller
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Letter |
Colossal injection of catalyst atoms into silicon nanowires
Aluminium catalyst is trapped during growth of a silicon nanowire from vapour phase at concentrations vastly beyond equilibrium solid solubility, but is homogeneously distributed as atoms and not found as clusters or precipitates; this is a potential route to tailoring the composition and properties of nanowires.
- Oussama Moutanabbir
- , Dieter Isheim
- & David N. Seidman
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Article |
Magnetic resonance fingerprinting
A new approach to magnetic resonance, ‘magnetic resonance fingerprinting', is reported, which combines a data acquisition scheme with a pattern-recognition algorithm that looks for the ‘fingerprints’ of interest within the data.
- Dan Ma
- , Vikas Gulani
- & Mark A. Griswold
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News & Views |
The fog clears
A technique has been developed to image a fluorescent object hiding behind a light-scattering screen without the need for a detector behind the screen. The approach could find applications in imaging biological tissue. See Letter p.232
- Demetri Psaltis
- & Ioannis N. Papadopoulos
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Visualizing heavy fermions emerging in a quantum critical Kondo lattice
A picture of how heavy fermions acquire their mass enhancement has now been obtained using scanning tunnelling spectroscopy.
- Pegor Aynajian
- , Eduardo H. da Silva Neto
- & Ali Yazdani
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Letter |
Imaging ultrafast molecular dynamics with laser-induced electron diffraction
Molecular structures are imaged with sub-ångström precision and exposure times of a few femtoseconds.
- Cosmin I. Blaga
- , Junliang Xu
- & C. D. Lin